Z10230
Z10002

NMR Reference Standards for 5mm Probes

  • Sale
  • Regular price $338.83


Certified NMR Reference Standard for full Operational Qualification of 5mm Bruker Probes.

Test Composition
1H lineshape to be used with RT probes at 200-300 MHz 3% Chloroform (CHCl3) 0.2% TMS in Acetone-d6.
1H lineshape 1% Chloroform (CHCl3) in Acetone-d6.
1H lineshape to be used with Cryoprobes and RT probes at 700 MHz or higher 0.3% Chloroform (CHCl3) in Acetone-d6.
1H Sensitivity 0.1% Ethylbenzene (EB) in Chloroform-d.
Water Suppression 2 mM Sucrose 0.5 mM DSS 2 mM NaN3 in H2O/D2O 90/10. Please
Water Suppression to be used with Cryoprobes and RT probes at 700 MHz or higher 2 mM Sucrose 0.5 mM DSS 2 mM NaN3 in H2O/D2O 90/10. Please
15N & 13C Pulse Calibration 100 mM 15N-enriched Urea 100 mM 13C-enriched Methanol in DMSO-d6.
13C Sensitivity & Resolution 40% Dioxane in Benzene-d6.
13C Sensitivity & 1H decoupling 10% Ethylbenzene (EB) in Chloroform-d.
31P Sensitivity 0.0485 M Triphenylphosphate (TPP) in Acetone-d6.
15N Sensitivity 90% Formamide in DMSO-d6.
19F Sensitivity 0.05% aaa-Trifluorotoluene (TFT) in Chloroform-d.
29Si Sensitivity 85% Hexamethyldisiloxane (HMDSO) in Benzene-d6.
Room Temperature Calibration - NMR Thermometer 99.8% Methanol-d4
High Temperature [300K - 380K] Calibration 80% Glycol in DMSO-d6.
Low temperature [180K - 300K] Calibration 4% Methanol (CH3OH) in Methanol-d4.
Gradient Recovery Test 0.1 mg GDCl3/ml D2O with 1% H2O + 0.1% CH3OH 13C.
2D experiments 25 mM Cyclosporine in Benzene-d6.
Water Suppression 2D 2 mM Lysozyme in H2O/D2O 90/10.
1D NOE Diff 100 mg Pamoic acid /ml DMSO-d6 + 1%TMS.