Z10230
Z10002

NMR Standard Reference Sample for 5mm Probes

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Certified NMR Reference Standard for full Operational Qualification of 5mm Bruker Probes.

Test Composition
1H lineshape to be used with RT probes at 200-300 MHz Z10230 3% Chloroform (CHCl3) 0.2% TMS in Acetone-d6, 5mm
1H lineshape Z10248 1% Chloroform (CHCl3) in Acetone-d6, 5mm
1H lineshape to be used with Cryoprobes and RT inverse probes at 700 MHz or higher Z10701 0.3% Chloroform (CHCl3) in Acetone-d6, 5mm
1H Sensitivity Z10120 0.1% Ethylbenzene (EB) in Chloroform-d, 5mm
Water Suppression Z10246 2 mM Sucrose 0.5 mM DSS 2 mM NaN3 in H2O/D2O 90/10, 5mm
Water Suppression to be used with Cryoprobes and RT inverse probes at 700 MHz or higher Z10902 2 mM Sucrose 0.5 mM DSS 2 mM NaN3 in H2O/D2O 90/10, 5mm
15N & 13C Pulse Calibration Z10263 100 mM 15N-enriched Urea 100 mM 13C-enriched Methanol in DMSO-d6, 5mm
13C Sensitivity & Resolution, ASTM
Z10163 40% Dioxane in Benzene-d6, 5mm
13C Sensitivity & 1H decoupling Z10153 10% Ethylbenzene (EB) in Chloroform-d, 5mm
31P Sensitivity Z10201 0.0485 M Triphenylphosphate (TPP) in Acetone-d6, 5mm
15N Sensitivity Z10187 90% Formamide in DMSO-d6, 5mm
19F Sensitivity Z10234 0.05% aaa-Trifluorotoluene (TFT) in Chloroform-d, 5mm
29Si Sensitivity Z10209 85% Hexamethyldisiloxane (HMDSO) in Benzene-d6 , 5mm
Temperature [282 K-330 K] Calibration - NMR Thermometer Z10627 99.8% Methanol-d4, 5mm
High Temperature [300 K - 380 K] Calibration Z10129 80% Glycol in DMSO-d6, 5mm
Low temperature [180 K - 300 K] Calibration Z10127 4% Methanol (CH3OH) in Methanol-d4, 5mm
Gradient Recovery Test Z10083 0.1 mg GDCl3/ml D2O with 1% H2O + 0.1% CH3OH 13C, 5mm
2D experiments Z10093 25 mM Cyclosporine in Benzene-d6, 5mm
Water Suppression 2D Z10241 2 mM Lysozyme in H2O/D2O 90/10, 5mm
1D NOE Diff Z10298 100 mg Pamoic acid /ml DMSO-d6 + 1%TMS, 5mm